Ultra-fast MAS

Magic angle spinning (MAS) is a commonly used method for improving resolution and sensitivity in solid-state NMR.

Our 1.3 mm magic angle spinning (MAS) probe can spin powder samples at speeds of up to 60 kHz. This leads to much narrower spectral line widths for nuclei such as 1H, allowing individual hydrogen sites to be resolved.

We use this probe to acquire high-resolution two-dimensional solid-state NMR spectra that show correlations between different1H sites, or between 1H and other nuclei such as 13C or 14N.

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